4LOV
Crystal structure of FimH in complex with Heptylmannoside
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | SOLEIL BEAMLINE PROXIMA 1 |
Synchrotron site | SOLEIL |
Beamline | PROXIMA 1 |
Temperature [K] | 100 |
Detector technology | PIXEL |
Collection date | 2012-12-08 |
Detector | DECTRIS PILATUS 6M |
Wavelength(s) | 0.9791 |
Spacegroup name | P 21 21 21 |
Unit cell lengths | 39.900, 41.820, 97.490 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 38.430 - 1.500 |
R-factor | 0.1625 |
Rwork | 0.161 |
R-free | 0.18960 |
Structure solution method | MOLECULAR REPLACEMENT |
RMSD bond length | 0.010 |
RMSD bond angle | 1.080 |
Data reduction software | XDS |
Data scaling software | XDS |
Phasing software | PHASER |
Refinement software | PHENIX ((phenix.refine: 1.8_1069)) |
Data quality characteristics
Overall | Inner shell | Outer shell | |
Low resolution limit [Å] | 40.000 | 38.444 | 1.673 |
High resolution limit [Å] | 1.499 | 3.200 | 1.499 |
Rmerge | 0.090 | ||
Number of reflections | 24894 | ||
Completeness [%] | 100.0 | 100 | 100 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 |