4LO7
HA70(D3)-HA17-HA33
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | APS BEAMLINE 24-ID-C |
Synchrotron site | APS |
Beamline | 24-ID-C |
Temperature [K] | 100 |
Detector technology | CCD |
Collection date | 2011-07-14 |
Detector | ADSC QUANTUM 315 |
Wavelength(s) | 0.97918 |
Spacegroup name | P 21 21 2 |
Unit cell lengths | 159.590, 187.490, 120.430 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 49.202 - 3.730 |
R-factor | 0.2691 |
Rwork | 0.268 |
R-free | 0.29320 |
Structure solution method | MOLECULAR REPLACEMENT |
RMSD bond length | 0.009 |
RMSD bond angle | 1.127 |
Data reduction software | MOSFLM |
Data scaling software | SCALA |
Phasing software | PHASES |
Refinement software | PHENIX ((phenix.refine: 1.7.2_869)) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 50.000 | 3.900 |
High resolution limit [Å] | 3.730 | 3.730 |
Rmerge | 0.119 | 0.656 |
Number of reflections | 38152 | |
<I/σ(I)> | 7.4 | 2.1 |
Completeness [%] | 99.7 | 100 |
Redundancy | 3.6 | 3.7 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | EVAPORATION | 8.2 | 292 | 0.1 M Tris, 0.1 M sodium chloride, 6% PEG2000, pH 8.2, EVAPORATION, temperature 292.0K |