4LO4
Apo HA-70
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | SSRL BEAMLINE BL7-1 |
Synchrotron site | SSRL |
Beamline | BL7-1 |
Temperature [K] | 100 |
Detector technology | CCD |
Collection date | 2011-11-02 |
Detector | ADSC QUANTUM 315r |
Wavelength(s) | 0.97952 |
Spacegroup name | I 41 3 2 |
Unit cell lengths | 261.750, 261.750, 261.750 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 44.890 - 2.871 |
R-factor | 0.1867 |
Rwork | 0.186 |
R-free | 0.20570 |
Structure solution method | MOLECULAR REPLACEMENT |
RMSD bond length | 0.005 |
RMSD bond angle | 0.913 |
Data reduction software | MOSFLM |
Data scaling software | SCALA |
Phasing software | PHASES |
Refinement software | PHENIX ((phenix.refine: 1.7.2_869)) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 50.000 | 3.000 |
High resolution limit [Å] | 2.871 | 2.871 |
Rmerge | 0.083 | 0.757 |
Number of reflections | 34988 | |
<I/σ(I)> | 14.8 | 2.3 |
Completeness [%] | 99.9 | 100 |
Redundancy | 7 | 6.6 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | EVAPORATION | 4.4 | 292 | 0.1 M sodium acetate, 1.5 M ammonium chloride, pH 4.4, EVAPORATION, temperature 292.0K |