4LO2
HA17-HA33-Lac
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | SSRL BEAMLINE BL11-1 |
Synchrotron site | SSRL |
Beamline | BL11-1 |
Temperature [K] | 100 |
Detector technology | PIXEL |
Collection date | 2012-01-14 |
Detector | DECTRIS PILATUS 6M |
Wavelength(s) | 0.97952 |
Spacegroup name | C 2 2 21 |
Unit cell lengths | 106.490, 119.153, 163.071 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 32.060 - 2.254 |
R-factor | 0.1686 |
Rwork | 0.166 |
R-free | 0.21080 |
Structure solution method | MOLECULAR REPLACEMENT |
RMSD bond length | 0.008 |
RMSD bond angle | 1.049 |
Data reduction software | HKL-2000 |
Data scaling software | HKL-2000 |
Phasing software | PHASES |
Refinement software | PHENIX ((phenix.refine: 1.7.2_869)) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 50.000 | 2.400 |
High resolution limit [Å] | 2.254 | 2.254 |
Rmerge | 0.057 | 0.384 |
Number of reflections | 47909 | |
<I/σ(I)> | 14.4 | 2 |
Completeness [%] | 97.4 | 98.9 |
Redundancy | 4.6 | 4.3 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | EVAPORATION | 6.2 | 292 | 0.1 M MES, 0.1 M magnesium chloride, 5% PEG8000, pH 6.2, EVAPORATION, temperature 292.0K |