4LMY
Structure of GAS PerR-Zn-Zn
Experimental procedure
| Experimental method | SINGLE WAVELENGTH |
| Source type | SYNCHROTRON |
| Source details | NSRRC BEAMLINE BL13B1 |
| Synchrotron site | NSRRC |
| Beamline | BL13B1 |
| Temperature [K] | 100 |
| Detector technology | CCD |
| Collection date | 2009-07-26 |
| Detector | NOIR-1 |
| Wavelength(s) | 1.0000 |
| Spacegroup name | P 1 21 1 |
| Unit cell lengths | 33.109, 87.496, 59.389 |
| Unit cell angles | 90.00, 94.78, 90.00 |
Refinement procedure
| Resolution | 21.169 - 1.600 |
| R-factor | 0.2213 |
| Rwork | 0.220 |
| R-free | 0.23890 |
| Structure solution method | MAD |
| RMSD bond length | 0.003 |
| RMSD bond angle | 0.789 |
| Data reduction software | d*TREK |
| Data scaling software | d*TREK |
| Phasing software | SOLVE |
| Refinement software | PHENIX ((phenix.refine: 1.8.2_1309)) |
Data quality characteristics
| Overall | Outer shell | |
| Low resolution limit [Å] | 30.000 | 1.550 |
| High resolution limit [Å] | 1.500 | 1.500 |
| Number of reflections | 51675 | |
| Completeness [%] | 95.6 | 79.7 |
| Redundancy | 4.8 | 3.7 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 | VAPOR DIFFUSION, HANGING DROP | 8.6 | 298 | 0.1M Tris, 0.25M magnesium chloride, 27% PEG 4000, pH 8.6, VAPOR DIFFUSION, HANGING DROP, temperature 298.0K |
| 1 | VAPOR DIFFUSION, HANGING DROP | 8.6 | 298 | 0.1M Tris, 0.25M magnesium chloride, 27% PEG 4000, pH 8.6, VAPOR DIFFUSION, HANGING DROP, temperature 298.0K |
