4LJN
Crystal Structure of MOZ double PHD finger
Experimental procedure
| Experimental method | SINGLE WAVELENGTH |
| Source type | SYNCHROTRON |
| Source details | ESRF BEAMLINE ID23-2 |
| Synchrotron site | ESRF |
| Beamline | ID23-2 |
| Temperature [K] | 100 |
| Detector technology | CCD |
| Collection date | 2011-07-04 |
| Detector | MARMOSAIC 225 mm CCD |
| Wavelength(s) | 0.8726 |
| Spacegroup name | P 31 2 1 |
| Unit cell lengths | 64.685, 64.685, 64.804 |
| Unit cell angles | 90.00, 90.00, 120.00 |
Refinement procedure
| Resolution | 56.019 - 3.000 |
| R-factor | 0.2288 |
| Rwork | 0.228 |
| R-free | 0.24250 |
| Structure solution method | MOLECULAR REPLACEMENT |
| Starting model (for MR) | 4lk9 |
| RMSD bond length | 0.010 |
| RMSD bond angle | 1.087 |
| Data reduction software | XDS |
| Data scaling software | SCALA (3.3.20) |
| Phasing software | PHASER |
| Refinement software | PHENIX (1.8_1069) |
Data quality characteristics
| Overall | Inner shell | Outer shell | |
| Low resolution limit [Å] | 56.019 | 56.019 | 3.160 |
| High resolution limit [Å] | 3.000 | 9.490 | 3.000 |
| Rmerge | 0.034 | 0.709 | |
| Total number of observations | 464 | 2180 | |
| Number of reflections | 3347 | ||
| <I/σ(I)> | 14.9 | 17.9 | 1 |
| Completeness [%] | 99.7 | 97.5 | 99.3 |
| Redundancy | 4.5 | 3.7 | 4.6 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 | VAPOR DIFFUSION | 7 | 293 | 60% tacsimate, pH 7, VAPOR DIFFUSION, temperature 293K |
