4LI4
Crystal structure of HCoV-OC43 N-NTD complexed with AMP
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | NSRRC BEAMLINE BL13B1 |
Synchrotron site | NSRRC |
Beamline | BL13B1 |
Temperature [K] | 100 |
Detector technology | CCD |
Collection date | 2011-12-12 |
Detector | ADSC QUANTUM 315r |
Wavelength(s) | 1 |
Spacegroup name | P 65 |
Unit cell lengths | 81.919, 81.919, 42.893 |
Unit cell angles | 90.00, 90.00, 120.00 |
Refinement procedure
Resolution | 26.814 - 1.710 |
R-factor | 0.2499 |
Rwork | 0.249 |
R-free | 0.26530 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 4j3k |
RMSD bond length | 0.018 |
RMSD bond angle | 2.228 |
Data reduction software | HKL-2000 |
Data scaling software | HKL-2000 |
Phasing software | CNS |
Refinement software | CNS |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 30.000 | |
High resolution limit [Å] | 1.710 | 1.710 |
Rmerge | 0.030 | |
Number of reflections | 17535 | |
Completeness [%] | 97.8 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, SITTING DROP | 7.5 | 293 | 2M SPG, 25% PEG1500, 5mM AMP, pH 7.5, VAPOR DIFFUSION, SITTING DROP, temperature 293K |