4LFZ
Crystal Structure of Frameshift Suppressor tRNA SufA6 Bound to Codon CCC-U in the Absence of Paromomycin
This is a non-PDB format compatible entry.
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | APS BEAMLINE 24-ID-E |
Synchrotron site | APS |
Beamline | 24-ID-E |
Temperature [K] | 100 |
Detector technology | CCD |
Collection date | 2012-04-22 |
Detector | ADSC QUANTUM 315 |
Wavelength(s) | 0.97 |
Spacegroup name | P 21 21 21 |
Unit cell lengths | 210.375, 451.022, 621.092 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 34.765 - 3.920 |
R-factor | 0.210119005126 |
Rwork | 0.208 |
R-free | 0.26504 |
Structure solution method | FOURIER SYNTHESIS |
RMSD bond length | 0.010 |
RMSD bond angle | 1.696 |
Data scaling software | XSCALE |
Refinement software | PHENIX |
Data quality characteristics
Overall | Inner shell | Outer shell | |
Low resolution limit [Å] | 34.800 | 3.900 | |
High resolution limit [Å] | 3.800 | 16.990 | 3.800 |
Rmerge | 0.338 | 0.016 | 0.016 |
Number of reflections | 573835 | 5898 | 42409 |
<I/σ(I)> | 5.5 | 23.13 | 1.18 |
Completeness [%] | 99.6 | 84.6 | 99.9 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION | 7 | 293 | 4% PEG 20k, 4% PEG550 MME, 0.1M TRIS-ACETATE, 0.2M KSCN, 10mM MgCl2, pH 7.0, vapor diffusion, temperature 293K |