4LFX
X-ray structure of the adduct between hen egg white lysozyme and Auoxo6, a dinuclear gold(III) complex with -dioxo bridges linking the two metal centers
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | ROTATING ANODE |
Source details | ENRAF-NONIUS FR571 |
Collection date | 2013-02-11 |
Wavelength(s) | 1.5418 |
Spacegroup name | P 43 21 2 |
Unit cell lengths | 78.269, 78.269, 37.208 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 30.880 - 2.100 |
R-factor | 0.204 |
Rwork | 0.204 |
R-free | 0.28100 |
Structure solution method | FOURIER SYNTHESIS |
RMSD bond length | 0.013 |
RMSD bond angle | 1.700 |
Data reduction software | HKL-2000 |
Data scaling software | HKL-2000 |
Phasing software | CNS |
Refinement software | CNS (1.3) |
Data quality characteristics
Overall | |
Low resolution limit [Å] | 30.880 |
High resolution limit [Å] | 2.100 |
Number of reflections | 6133 |
Completeness [%] | 86.2 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 |