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4LFN

Crystal Structure of D-galactose-6-phosphate isomerase in complex with D-ribulose

Experimental procedure
Experimental methodSINGLE WAVELENGTH
Source typeSYNCHROTRON
Source detailsPAL/PLS BEAMLINE 7A (6B, 6C1)
Synchrotron sitePAL/PLS
Beamline7A (6B, 6C1)
Temperature [K]100
Detector technologyCCD
Collection date2012-06-26
DetectorADSC QUANTUM 270
Wavelength(s)0.97932
Spacegroup nameP 21 21 2
Unit cell lengths108.261, 116.009, 54.752
Unit cell angles90.00, 90.00, 90.00
Refinement procedure
Resolution50.000 - 1.650
Rwork0.241
R-free0.25870
Structure solution methodMOLECULAR REPLACEMENT
Starting model (for MR)4lfk
Data reduction softwareHKL-2000
Data scaling softwareSCALEPACK
Phasing softwareCNS
Refinement softwareCNS
Data quality characteristics
 OverallInner shellOuter shell
Low resolution limit [Å]50.00050.0001.680
High resolution limit [Å]1.6504.4801.650
Rmerge0.1020.0690.597
Number of reflections82263
<I/σ(I)>8.2
Completeness [%]97.988.695.9
Redundancy12.311.710.3
Crystallization Conditions
crystal IDmethodpHtemperaturedetails
1VAPOR DIFFUSION, HANGING DROP29520% PEG 3350, 0.2M potassium formate, VAPOR DIFFUSION, HANGING DROP, temperature 295K

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