4LDG
Crystal Structure of CpSET8 from Cryptosporidium, cgd4_370
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | CLSI BEAMLINE 08ID-1 |
Synchrotron site | CLSI |
Beamline | 08ID-1 |
Temperature [K] | 100 |
Detector technology | CCD |
Collection date | 2013-05-23 |
Detector | MARMOSAIC 300 mm CCD |
Wavelength(s) | 0.97949 |
Spacegroup name | P 41 21 2 |
Unit cell lengths | 68.229, 68.229, 142.694 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 49.360 - 2.310 |
R-factor | 0.1953 |
Rwork | 0.194 |
R-free | 0.22720 |
Structure solution method | MOLECULAR REPLACEMENT |
RMSD bond length | 0.010 |
RMSD bond angle | 1.382 |
Data reduction software | DENZO |
Data scaling software | SCALEPACK |
Phasing software | BALBES |
Refinement software | REFMAC |
Data quality characteristics
Overall | Inner shell | Outer shell | |
Low resolution limit [Å] | 50.000 | 50.000 | 2.340 |
High resolution limit [Å] | 2.300 | 6.240 | 2.300 |
Rmerge | 0.144 | 0.095 | 0.979 |
Number of reflections | 15678 | ||
<I/σ(I)> | 10.5 | 3.21 | |
Completeness [%] | 100.0 | 99.7 | 100 |
Redundancy | 10.3 | 9 | 10.6 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, SITTING DROP | 7.5 | 293 | 1.8 M Na Malonate, 20 % PEG 3350, 7% butanol, 20 glycerol, pH 7.5, VAPOR DIFFUSION, SITTING DROP, temperature 293K |