4LDF
Crystal Structure of CpBRD2 from cryptosporidium, cgd3_3190
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | ROTATING ANODE |
Source details | RIGAKU FR-E+ SUPERBRIGHT |
Temperature [K] | 100 |
Detector technology | IMAGE PLATE |
Collection date | 2013-04-29 |
Detector | RIGAKU RAXIS IV |
Wavelength(s) | 1.54178 |
Spacegroup name | P 1 21 1 |
Unit cell lengths | 37.892, 44.642, 59.537 |
Unit cell angles | 90.00, 96.50, 90.00 |
Refinement procedure
Resolution | 33.530 - 2.000 |
R-factor | 0.1864 |
Rwork | 0.184 |
R-free | 0.22550 |
Structure solution method | MOLECULAR REPLACEMENT |
RMSD bond length | 0.010 |
RMSD bond angle | 1.010 |
Data reduction software | DENZO |
Data scaling software | SCALEPACK |
Phasing software | PHASER (2.5.1) |
Refinement software | BUSTER-TNT |
Data quality characteristics
Overall | Inner shell | Outer shell | |
Low resolution limit [Å] | 50.000 | 50.000 | 2.030 |
High resolution limit [Å] | 2.000 | 5.430 | 2.000 |
Rmerge | 0.118 | 0.052 | 0.756 |
Number of reflections | 13557 | ||
<I/σ(I)> | 7.3 | ||
Completeness [%] | 99.9 | 99 | 99.4 |
Redundancy | 3.4 | 3.4 | 3.3 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, SITTING DROP | 7.5 | 293 | 30 % PEG 2K MME 0.1 M Potassium thiocyanate 15% glycerol, pH 7.5, VAPOR DIFFUSION, SITTING DROP, temperature 293K |