4L8J
Crystal structure of a Putative efflux transporter (BACEGG_01895) from Bacteroides eggerthii DSM 20697 at 2.06 A resolution
Experimental procedure
Experimental method | MAD |
Source type | SYNCHROTRON |
Source details | SSRL BEAMLINE BL11-1 |
Synchrotron site | SSRL |
Beamline | BL11-1 |
Temperature [K] | 100 |
Detector technology | PIXEL |
Collection date | 2013-05-02 |
Detector | DECTRIS PILATUS 6M |
Wavelength(s) | 0.97871, 0.91837, 0.97817 |
Spacegroup name | P 41 21 2 |
Unit cell lengths | 69.536, 69.536, 187.676 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 46.486 - 2.060 |
R-factor | 0.2093 |
Rwork | 0.208 |
R-free | 0.23440 |
Structure solution method | MAD |
RMSD bond length | 0.010 |
RMSD bond angle | 1.040 |
Data reduction software | XDS |
Data scaling software | XSCALE (July 4, 2012) |
Phasing software | SHELX |
Refinement software | BUSTER-TNT (2.10.0) |
Data quality characteristics
Overall | Inner shell | Outer shell | |
Low resolution limit [Å] | 46.486 | 2.130 | |
High resolution limit [Å] | 2.060 | 4.420 | 2.060 |
Rmerge | 0.076 | 0.037 | 0.884 |
Number of reflections | 29410 | 3239 | 2727 |
<I/σ(I)> | 14.77 | 37.9 | 2.2 |
Completeness [%] | 99.8 | 99.2 | 99.9 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, SITTING DROP | 9.83 | 277 | 12.0% polyethylene glycol 8000, 0.1M sodium chloride, 0.1M CAPS pH 9.83, NANODROP, VAPOR DIFFUSION, SITTING DROP, temperature 277K |