4L63
Apo form of AB5 holotoxin
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | AUSTRALIAN SYNCHROTRON BEAMLINE MX2 |
Synchrotron site | Australian Synchrotron |
Beamline | MX2 |
Temperature [K] | 100 |
Detector technology | CCD |
Collection date | 2011 |
Detector | ADSC QUANTUM 315r |
Wavelength(s) | 0.953699 |
Spacegroup name | P 65 2 2 |
Unit cell lengths | 120.530, 120.530, 273.510 |
Unit cell angles | 90.00, 90.00, 120.00 |
Refinement procedure
Resolution | 45.211 - 1.800 |
R-factor | 0.1781 |
Rwork | 0.177 |
R-free | 0.19730 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 2wv6 |
RMSD bond length | 0.007 |
RMSD bond angle | 1.093 |
Data reduction software | MOSFLM |
Data scaling software | SCALA |
Phasing software | PHASER |
Refinement software | PHENIX ((phenix.refine: 1.8.1_1168)) |
Data quality characteristics
Overall | |
Low resolution limit [Å] | 39.500 |
High resolution limit [Å] | 1.800 |
Rmerge | 0.072 |
Number of reflections | 109241 |
<I/σ(I)> | 8.2 |
Completeness [%] | 99.9 |
Redundancy | 11.9 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 4.5 | 295 | 0.1M HEPES and 0.6M Na/K/PO4, VAPOR DIFFUSION, HANGING DROP, temperature 295K, pH 4.5 |