4L57
High resolutin structure of human cytosolic 5'(3')-deoxyribonucleotidase
Experimental procedure
| Experimental method | SINGLE WAVELENGTH |
| Source type | SYNCHROTRON |
| Source details | BESSY BEAMLINE 14.2 |
| Synchrotron site | BESSY |
| Beamline | 14.2 |
| Temperature [K] | 100 |
| Detector technology | CCD |
| Collection date | 2010-02-03 |
| Detector | MARMOSAIC 225 mm CCD |
| Spacegroup name | P 1 |
| Unit cell lengths | 39.128, 46.493, 61.409 |
| Unit cell angles | 68.16, 81.47, 75.28 |
Refinement procedure
| Resolution | 22.480 - 1.080 |
| R-factor | 0.1436 |
| Rwork | 0.144 |
| R-free | 0.18300 |
| Structure solution method | FOURIER SYNTHESIS |
| Refinement software | SHELX |
Data quality characteristics
| Overall | |
| Low resolution limit [Å] | 23.400 |
| High resolution limit [Å] | 1.080 |
| Number of reflections | 142636 |
| Completeness [%] | 98.9 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 | 4.2 | 291 | 40MM KH2PO4, 5% PEG 8000, 20% GLYCEROL, pH 4.2, VAPOR DIFFUSION, temperature 291K |
