4L57
High resolutin structure of human cytosolic 5'(3')-deoxyribonucleotidase
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | BESSY BEAMLINE 14.2 |
Synchrotron site | BESSY |
Beamline | 14.2 |
Temperature [K] | 100 |
Detector technology | CCD |
Collection date | 2010-02-03 |
Detector | MARMOSAIC 225 mm CCD |
Spacegroup name | P 1 |
Unit cell lengths | 39.128, 46.493, 61.409 |
Unit cell angles | 68.16, 81.47, 75.28 |
Refinement procedure
Resolution | 22.480 - 1.080 |
R-factor | 0.1436 |
Rwork | 0.144 |
R-free | 0.18300 |
Structure solution method | FOURIER SYNTHESIS |
Refinement software | SHELX |
Data quality characteristics
Overall | |
Low resolution limit [Å] | 23.400 |
High resolution limit [Å] | 1.080 |
Number of reflections | 142636 |
Completeness [%] | 98.9 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | 4.2 | 291 | 40MM KH2PO4, 5% PEG 8000, 20% GLYCEROL, pH 4.2, VAPOR DIFFUSION, temperature 291K |