4L1H
Bence-Jones immunoglobulin REI variable portion with seven point mutations
Experimental procedure
| Experimental method | SINGLE WAVELENGTH |
| Source type | SYNCHROTRON |
| Source details | EMBL/DESY, HAMBURG BEAMLINE X11 |
| Synchrotron site | EMBL/DESY, Hamburg |
| Beamline | X11 |
| Detector technology | IMAGE PLATE |
| Detector | MAR555 FLAT PANEL |
| Wavelength(s) | 0.98 |
| Spacegroup name | P 61 2 2 |
| Unit cell lengths | 87.143, 87.143, 73.366 |
| Unit cell angles | 90.00, 90.00, 120.00 |
Refinement procedure
| Resolution | 52.610 - 1.680 |
| R-factor | 0.1952 |
| Rwork | 0.195 |
| R-free | 0.26000 |
| Structure solution method | MOLECULAR REPLACEMENT |
| Refinement software | SHELXL-97 |
Data quality characteristics
| Overall | Outer shell | |
| Low resolution limit [Å] | 52.610 | |
| High resolution limit [Å] | 1.680 | 1.680 |
| Number of reflections | 15847 | |
| Completeness [%] | 99.8 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 |
