4L16
Crystal structure of FIGL-1 AAA domain in complex with ADP
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | SSRF BEAMLINE BL17U |
Synchrotron site | SSRF |
Beamline | BL17U |
Temperature [K] | 100 |
Detector technology | CCD |
Collection date | 2010-12-26 |
Detector | MARMOSAIC 325 mm CCD |
Spacegroup name | P 65 |
Unit cell lengths | 113.539, 113.539, 58.101 |
Unit cell angles | 90.00, 90.00, 120.00 |
Refinement procedure
Resolution | 37.164 - 2.800 |
R-factor | 0.2015 |
Rwork | 0.200 |
R-free | 0.23890 |
Structure solution method | MOLECULAR REPLACEMENT |
RMSD bond length | 0.010 |
RMSD bond angle | 1.309 |
Data reduction software | HKL-2000 |
Data scaling software | HKL-2000 |
Phasing software | PHASES |
Refinement software | PHENIX ((phenix.refine: 1.6.4_486)) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 37.200 | 2.900 |
High resolution limit [Å] | 2.800 | 2.800 |
Number of reflections | 10055 | |
Completeness [%] | 96.4 | 84 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 6.5 | 293 | 0.1M Bis-Tris, 0.5 M Sodium acetate, pH 6.5, VAPOR DIFFUSION, HANGING DROP, temperature 293K |