4L15
Crystal structure of FIGL-1 AAA domain
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | ROTATING ANODE |
Source details | RIGAKU MICROMAX-007 HF |
Temperature [K] | 100 |
Detector technology | IMAGE PLATE |
Detector | RIGAKU RAXIS IV++ |
Wavelength(s) | 1.5418 |
Spacegroup name | P 65 |
Unit cell lengths | 108.295, 108.295, 54.870 |
Unit cell angles | 90.00, 90.00, 120.00 |
Refinement procedure
Resolution | 38.541 - 2.600 |
R-factor | 0.1884 |
Rwork | 0.186 |
R-free | 0.22400 |
Structure solution method | MOLECULAR REPLACEMENT |
RMSD bond length | 0.009 |
RMSD bond angle | 1.186 |
Data reduction software | HKL-2000 |
Data scaling software | HKL-2000 |
Phasing software | PHASES |
Refinement software | PHENIX ((phenix.refine: 1.6.4_486)) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 38.541 | 2.690 |
High resolution limit [Å] | 2.600 | 2.600 |
Number of reflections | 11481 | |
Completeness [%] | 97.4 | 100 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, SITTING DROP | 7 | 293 | 0.1M Tris-HCl, 0.5 M sodium malonate, 0.3% PEG 10,000, pH 7.0, VAPOR DIFFUSION, SITTING DROP, temperature 293K |