Experimental procedure
| Experimental method | SINGLE WAVELENGTH |
| Source type | SYNCHROTRON |
| Source details | SSRL BEAMLINE BL9-2 |
| Synchrotron site | SSRL |
| Beamline | BL9-2 |
| Temperature [K] | 96 |
| Detector technology | CCD |
| Collection date | 2001-06-23 |
| Detector | ADSC |
| Wavelength(s) | 0.775 |
| Spacegroup name | I 2 2 2 |
| Unit cell lengths | 49.910, 70.528, 80.359 |
| Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
| Resolution | 25.041 - 1.098 |
| R-factor | 0.1137 |
| Rwork | 0.113 |
| R-free | 0.11830 |
| Structure solution method | MOLECULAR REPLACEMENT |
| Starting model (for MR) | 1eqw |
| RMSD bond length | 0.009 |
| RMSD bond angle | 1.367 |
| Data reduction software | DENZO |
| Data scaling software | SCALEPACK |
| Refinement software | PHENIX ((phenix.refine: 1.8.2_1309)) |
Data quality characteristics
| Overall | Outer shell | |
| Low resolution limit [Å] | 30.000 | 1.140 |
| High resolution limit [Å] | 1.098 | 1.098 |
| Rmerge | 0.070 | 0.395 |
| Number of reflections | 56763 | |
| <I/σ(I)> | 24.3 | 4.8 |
| Completeness [%] | 98.0 | 97.5 |
| Redundancy | 6.55 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 | VAPOR DIFFUSION, HANGING DROP | 7.5 | 298 | 2 M ammonium sulfate, 150 mM potassium chloride, pH 7.5, VAPOR DIFFUSION, HANGING DROP, temperature 298K |
