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4KRU

X-ray structure of catalytic domain of endolysin from clostridium perfringens phage phiSM101

Experimental procedure
Experimental methodSINGLE WAVELENGTH
Source typeROTATING ANODE
Source detailsRIGAKU MICROMAX-007 HF
Temperature [K]100
Detector technologyIMAGE PLATE
Collection date2012-09-27
DetectorRIGAKU RAXIS VII
Wavelength(s)1.5418
Spacegroup nameP 21 21 21
Unit cell lengths47.770, 57.620, 73.420
Unit cell angles90.00, 90.00, 90.00
Refinement procedure
Resolution30.960 - 1.370
R-factor0.172
Rwork0.172
R-free0.19300
Structure solution methodMOLECULAR REPLACEMENT
Starting model (for MR)1jfx
RMSD bond length0.005
RMSD bond angle1.400
Data reduction softwareCrystalClear
Data scaling softwareCrystalClear
Phasing softwareMOLREP
Refinement softwareCNS (1.3)
Data quality characteristics
 OverallOuter shell
Low resolution limit [Å]30.9601.420
High resolution limit [Å]1.3701.370
Rmerge0.0240.071
Number of reflections42675
<I/σ(I)>42.511.7
Completeness [%]98.485
Redundancy6.152.52
Crystallization Conditions
crystal IDmethodpHtemperaturedetails
1VAPOR DIFFUSION, SITTING DROP4.229320% PEG 3000, 0.2M Lithium sulphate, 0.1M phosphate-citrate, pH 4.2, VAPOR DIFFUSION, SITTING DROP, temperature 293K

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