4KPU
Electron transferring flavoprotein of Acidaminococcus fermentans: Towards a mechanism of flavin-based electron bifurcation
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | SLS BEAMLINE X10SA |
Synchrotron site | SLS |
Beamline | X10SA |
Detector technology | PIXEL |
Detector | PSI PILATUS 6M |
Spacegroup name | P 21 21 21 |
Unit cell lengths | 80.180, 84.890, 106.730 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 45.000 - 1.600 |
R-factor | 0.16283 |
Rwork | 0.161 |
R-free | 0.19072 |
Structure solution method | MAD |
RMSD bond length | 0.023 |
RMSD bond angle | 2.291 |
Data reduction software | XDS |
Data scaling software | XSCALE |
Phasing software | SHARP |
Refinement software | REFMAC (5.7.0032) |
Data quality characteristics
Overall | |
Low resolution limit [Å] | 45.000 |
High resolution limit [Å] | 1.600 |
Number of reflections | 90032 |
Completeness [%] | 98.0 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, SITTING DROP | 7.5 | 277 | 18% PEG, 0.1M BIS-Tris propane, 0.1M Na formate, 1mM FAD, pH 7.5, VAPOR DIFFUSION, SITTING DROP, temperature 277K |