4KPG
Crystal structure of MycP1 from the ESX-1 type VII secretion system
Experimental procedure
| Source type | SYNCHROTRON |
| Source details | CLSI BEAMLINE 08B1-1 |
| Synchrotron site | CLSI |
| Beamline | 08B1-1 |
| Detector technology | CCD |
| Collection date | 2011-08-15 |
| Detector | RAYONIX MX-300 |
| Wavelength(s) | 0.97895 |
| Spacegroup name | I 2 2 2 |
| Unit cell lengths | 81.000, 94.080, 119.600 |
| Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
| Resolution | 47.040 - 2.148 |
| R-factor | 0.1676 |
| Rwork | 0.166 |
| R-free | 0.19670 |
| Structure solution method | SAD |
| RMSD bond length | 0.007 |
| RMSD bond angle | 1.049 |
| Data scaling software | SCALA (CCP4_3.3.16) |
| Refinement software | PHENIX (1.7.2_869) |
Data quality characteristics
| Overall | |
| Low resolution limit [Å] | 59.930 |
| High resolution limit [Å] | 2.148 |
| Number of reflections | 25383 |
| Completeness [%] | 99.8 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 | VAPOR DIFFUSION, SITTING DROP | 7.5 | 293 | 0.2 M NaF, 25% PEG 3350, pH 7.5, VAPOR DIFFUSION, SITTING DROP, temperature 293K |
