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4KO8

Structure of p97 N-D1 R155H mutant in complex with ATPgS

Experimental procedure
Experimental methodSINGLE WAVELENGTH
Source typeSYNCHROTRON
Source detailsAPS BEAMLINE 22-ID
Synchrotron siteAPS
Beamline22-ID
Temperature [K]100
Detector technologyCCD
Collection date2005-10-01
DetectorMARMOSAIC 300 mm CCD
Wavelength(s)1
Spacegroup nameH 3
Unit cell lengths134.206, 134.206, 182.886
Unit cell angles90.00, 90.00, 120.00
Refinement procedure
Resolution98.110 - 1.980
R-factor0.19493
Rwork0.194
R-free0.20504
Structure solution methodMOLECULAR REPLACEMENT
RMSD bond length0.007
RMSD bond angle1.092
Data reduction softwareDENZO
Data scaling softwareSCALEPACK
Phasing softwareMOLREP
Refinement softwareREFMAC (5.5.0102)
Data quality characteristics
 OverallOuter shell
Low resolution limit [Å]100.0002.050
High resolution limit [Å]1.9801.980
Number of reflections79692
Completeness [%]100.0
Crystallization Conditions
crystal IDmethodpHtemperaturedetails
1VAPOR DIFFUSION, HANGING DROP5.6288100mM citrate buffer pH 5.6, 6% benzamidine, 7% PEG3350, and 20% glycerol, VAPOR DIFFUSION, HANGING DROP, temperature 288K

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