4KM8
Crystal structure of Sufud60
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | SSRF BEAMLINE BL17U |
Synchrotron site | SSRF |
Beamline | BL17U |
Temperature [K] | 100 |
Detector technology | CCD |
Collection date | 2012-06-29 |
Wavelength(s) | 1.000 |
Spacegroup name | C 2 2 21 |
Unit cell lengths | 76.276, 122.452, 118.611 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 50.000 - 2.260 |
R-factor | 0.21457 |
Rwork | 0.212 |
R-free | 0.25861 |
RMSD bond length | 0.013 |
RMSD bond angle | 1.337 |
Data reduction software | DENZO |
Data scaling software | SCALEPACK |
Refinement software | REFMAC (5.5.0102) |
Data quality characteristics
Overall | Inner shell | Outer shell | |
Low resolution limit [Å] | 50.000 | 50.000 | 2.330 |
High resolution limit [Å] | 2.250 | 4.850 | 2.250 |
Rmerge | 0.136 | 0.117 | 0.517 |
Number of reflections | 26211 | ||
<I/σ(I)> | 12.9 | ||
Completeness [%] | 99.2 | 97.7 | 99.5 |
Redundancy | 7.4 | 7 | 7.5 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 287 | 8% PEG 3350, 0.15M Ammonium Tartrate, vapor diffusion, hanging drop, temperature 287K |