4KKR
Crystal structure of Vibrio cholerae RbmA (crystal form 3)
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | CHESS BEAMLINE A1 |
Synchrotron site | CHESS |
Beamline | A1 |
Temperature [K] | 100 |
Detector technology | CCD |
Collection date | 2013-03-07 |
Detector | ADSC QUANTUM 210 |
Wavelength(s) | 0.9771 |
Spacegroup name | P 41 21 2 |
Unit cell lengths | 119.404, 119.404, 104.025 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 44.284 - 2.000 |
R-factor | 0.1619 |
Rwork | 0.161 |
R-free | 0.19160 |
Structure solution method | MOLECULAR REPLACEMENT |
RMSD bond length | 0.007 |
RMSD bond angle | 1.042 |
Data reduction software | HKL-2000 |
Data scaling software | HKL-2000 |
Phasing software | PHENIX |
Refinement software | PHENIX ((phenix.refine: 1.8.1_1168)) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 50.000 | 2.070 |
High resolution limit [Å] | 2.000 | 2.000 |
Number of reflections | 51215 | |
Completeness [%] | 99.9 | 99.7 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 5.5 | 294 | 0.1 M BIS-TRIS, 3.0 M NaCl, 25% Xylitol, 0.16% Thiamine monophosphate chlroide dihydrate, 0.16% Acetylsalicylic acid, 0.16% Cholic acid, 0.16% 1,2,3-Heptanetriol, 0.16% Vanillin, 0.16% N-Acetly-D-mannosamine, 0.02 M HEPES sodium, pH 5.5, VAPOR DIFFUSION, HANGING DROP, temperature 294K |