4KK5
Structure of the CLC-ec1 deltaNC construct in 20mM fluoride and 20mM bromide
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | ALS BEAMLINE 8.2.1 |
Synchrotron site | ALS |
Beamline | 8.2.1 |
Temperature [K] | 77 |
Detector technology | CCD |
Detector | ADSC QUANTUM 315r |
Wavelength(s) | 0.919 |
Spacegroup name | C 1 2 1 |
Unit cell lengths | 229.127, 98.166, 169.761 |
Unit cell angles | 90.00, 131.73, 90.00 |
Refinement procedure
Resolution | 39.782 - 3.171 |
R-factor | 0.2339 |
Rwork | 0.232 |
R-free | 0.27130 |
Structure solution method | MOLECULAR REPLACEMENT |
RMSD bond length | 0.006 |
RMSD bond angle | 0.814 |
Data reduction software | HKL-2000 |
Data scaling software | HKL-2000 |
Phasing software | PHASER |
Refinement software | PHENIX ((phenix.refine: 1.8.1_1168)) |
Data quality characteristics
Overall | |
Low resolution limit [Å] | 40.000 |
High resolution limit [Å] | 3.170 |
Number of reflections | 91572 |
Completeness [%] | 98.8 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 9 | 295 | 100mM Na/K tartrate, 26%PEG400, 100mM Glycine, pH 9.0, VAPOR DIFFUSION, HANGING DROP, temperature 295K |