4KF4
Crystal Structure of sfCherry
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | ALS BEAMLINE 5.0.2 |
Synchrotron site | ALS |
Beamline | 5.0.2 |
Temperature [K] | 100 |
Detector technology | CCD |
Collection date | 2011-05-04 |
Detector | ADSC QUANTUM 315r |
Wavelength(s) | 1.0 |
Spacegroup name | P 1 21 1 |
Unit cell lengths | 85.105, 96.294, 105.957 |
Unit cell angles | 90.00, 104.56, 90.00 |
Refinement procedure
Resolution | 45.260 - 1.994 |
R-factor | 0.2232 |
Rwork | 0.222 |
R-free | 0.26480 |
Structure solution method | MOLECULAR REPLACEMENT |
RMSD bond length | 0.008 |
RMSD bond angle | 1.059 |
Data reduction software | HKL-2000 |
Data scaling software | HKL-2000 |
Phasing software | PHASES |
Refinement software | PHENIX ((phenix.refine: dev_1338)) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 60.000 | 2.030 |
High resolution limit [Å] | 1.994 | 2.000 |
Rmerge | 0.095 | 0.546 |
Number of reflections | 97672 | |
<I/σ(I)> | 10.45 | 1.65 |
Completeness [%] | 97.0 | 98.1 |
Redundancy | 2.3 | 2.2 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, SITTING DROP | 5 | 298 | 0.1 M SPG buffer pH 5.0, 25 % PEG 1500, VAPOR DIFFUSION, SITTING DROP, temperature 298K |