4KEZ
Crystal structure of SsoPox W263F
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | SOLEIL BEAMLINE PROXIMA 1 |
Synchrotron site | SOLEIL |
Beamline | PROXIMA 1 |
Temperature [K] | 100 |
Detector technology | PIXEL |
Collection date | 2012-04-07 |
Detector | DECTRIS PILATUS 6M |
Wavelength(s) | 1.00882 |
Spacegroup name | P 21 21 21 |
Unit cell lengths | 87.130, 103.620, 151.660 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 49.030 - 1.850 |
R-factor | 0.153 |
Rwork | 0.151 |
R-free | 0.18640 |
Structure solution method | MOLECULAR REPLACEMENT |
RMSD bond length | 0.004 |
RMSD bond angle | 0.896 |
Refinement software | REFMAC |
Data quality characteristics
Overall | |
Low resolution limit [Å] | 49.030 |
High resolution limit [Å] | 1.850 |
Number of reflections | 117479 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 8 | 277 | 50 mM Tris-HCl, 23-25% PEG8000, pH 8.0, VAPOR DIFFUSION, HANGING DROP, temperature 277K |