4KC5
Crystal structure of the C-terminal part of RhiE from Burkholderia rhizoxinica
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | SLS BEAMLINE X06DA |
Synchrotron site | SLS |
Beamline | X06DA |
Temperature [K] | 100 |
Detector technology | PIXEL |
Collection date | 2012-10-22 |
Detector | DECTRIS PILATUS 2M-F |
Wavelength(s) | 1.0000 |
Spacegroup name | P 1 21 1 |
Unit cell lengths | 125.510, 144.130, 131.300 |
Unit cell angles | 90.00, 96.65, 90.00 |
Refinement procedure
Resolution | 48.350 - 2.140 |
R-factor | 0.18213 |
Rwork | 0.181 |
R-free | 0.22716 |
Structure solution method | MOLECULAR REPLACEMENT |
RMSD bond length | 0.015 |
RMSD bond angle | 1.550 |
Data reduction software | XDS |
Data scaling software | XSCALE |
Phasing software | PHASER |
Refinement software | REFMAC (5.7.0027) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 50.000 | 2.200 |
High resolution limit [Å] | 2.140 | 2.140 |
Number of reflections | 252811 | |
<I/σ(I)> | 2.02 | |
Completeness [%] | 99.2 | 97.8 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 8.5 | 293 | 20% (w/v) PEG 2000 MME, 100 mM Tris/HCl pH 8.5, 100 mM Trismethylamine, VAPOR DIFFUSION, HANGING DROP, temperature 293K |