Experimental procedure
| Experimental method | SINGLE WAVELENGTH |
| Source type | SYNCHROTRON |
| Source details | NSRRC BEAMLINE BL13B1 |
| Synchrotron site | NSRRC |
| Beamline | BL13B1 |
| Temperature [K] | 100 |
| Detector technology | CCD |
| Collection date | 2011-03-21 |
| Detector | ADSC QUANTUM 315r |
| Wavelength(s) | 0.97898 |
| Spacegroup name | P 31 |
| Unit cell lengths | 78.493, 78.493, 50.409 |
| Unit cell angles | 90.00, 90.00, 120.00 |
Refinement procedure
| Resolution | 25.693 - 2.200 |
| R-factor | 0.2004 |
| Rwork | 0.194 |
| R-free | 0.25090 |
| Structure solution method | SAD |
| RMSD bond length | 0.008 |
| RMSD bond angle | 1.142 |
| Data reduction software | HKL-2000 |
| Data scaling software | HKL-2000 |
| Phasing software | CNS |
| Refinement software | CNS |
Data quality characteristics
| Overall | Outer shell | |
| Low resolution limit [Å] | 30.000 | |
| High resolution limit [Å] | 2.200 | 2.200 |
| Number of reflections | 17389 | |
| Completeness [%] | 90.0 | 100 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 | VAPOR DIFFUSION, SITTING DROP | 8 | 298 | Tris 8.0, 20% PEG 3350 MME, VAPOR DIFFUSION, SITTING DROP, temperature 100K, temperature 298K |
