4KBC
CK1d in complex with {4-[3-(4-FLUOROPHENYL)-1H-PYRAZOL-4-YL]PYRIDIN-2-YL}METHANOL inhibitor
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | APS BEAMLINE 17-ID |
Synchrotron site | APS |
Beamline | 17-ID |
Detector technology | CCD |
Detector | ADSC QUANTUM 210 |
Spacegroup name | P 1 21 1 |
Unit cell lengths | 56.580, 118.140, 61.220 |
Unit cell angles | 90.00, 109.23, 90.00 |
Refinement procedure
Resolution | 19.960 - 1.980 |
R-factor | 0.1864 |
Rwork | 0.185 |
R-free | 0.21460 |
Structure solution method | MOLECULAR REPLACEMENT |
RMSD bond length | 0.010 |
RMSD bond angle | 1.000 |
Refinement software | BUSTER (2.11.5) |
Data quality characteristics
Overall | |
Low resolution limit [Å] | 56.580 |
High resolution limit [Å] | 1.980 |
Rmerge | 0.075 |
Number of reflections | 49525 |
<I/σ(I)> | 20 |
Completeness [%] | 96.3 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 |