4K5U
Recognition of the BG-H Antigen by a Lamprey Variable Lymphocyte Receptor
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | ROTATING ANODE |
Source details | RIGAKU |
Temperature [K] | 100 |
Detector technology | IMAGE PLATE |
Collection date | 2012-10-01 |
Detector | RIGAKU RAXIS IV++ |
Wavelength(s) | 1.5418 |
Spacegroup name | P 1 |
Unit cell lengths | 57.710, 62.784, 63.366 |
Unit cell angles | 72.03, 71.39, 84.35 |
Refinement procedure
Resolution | 59.720 - 1.698 |
R-factor | 0.20566 |
Rwork | 0.206 |
R-free | 0.24661 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 3e6j |
RMSD bond length | 0.028 |
RMSD bond angle | 2.220 |
Data reduction software | CrystalClear ((Rigaku)) |
Data scaling software | CrystalClear ((Rigaku)) |
Phasing software | AMoRE |
Refinement software | REFMAC (5.5.0102) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 59.720 | 1.760 |
High resolution limit [Å] | 1.698 | 1.698 |
Number of reflections | 82662 | |
Completeness [%] | 93.3 | 87.8 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 7 | 298 | 28.5% (w/v) PEG 3350, 0.6 M NaCl, and 0.1M Tris-HCl (pH 7.0), VAPOR DIFFUSION, HANGING DROP, temperature 298K |