4K4D
X-ray crystal structure of E. coli YbdB complexed with 2,4-dihydroxyphenacyl-CoA
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | ROTATING ANODE |
Source details | RIGAKU RU300 |
Temperature [K] | 100 |
Detector technology | IMAGE PLATE |
Collection date | 2008-12-28 |
Detector | RIGAKU RAXIS IV |
Wavelength(s) | 1.5418 |
Spacegroup name | P 21 21 2 |
Unit cell lengths | 59.664, 86.263, 50.250 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 20.400 - 2.170 |
R-factor | 0.1961 |
Rwork | 0.193 |
R-free | 0.25320 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 1vh9 |
RMSD bond length | 0.008 |
RMSD bond angle | 1.569 |
Data reduction software | DENZO |
Data scaling software | SCALEPACK |
Phasing software | MOLREP |
Refinement software | PHENIX ((phenix.refine: 1.8_1069)) |
Data quality characteristics
Overall | |
Low resolution limit [Å] | 20.400 |
High resolution limit [Å] | 2.170 |
Number of reflections | 14243 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 7 | 290 | 2.0 M SODIUM MALONATE, pH 7.0, VAPOR DIFFUSION, HANGING DROP, temperature 290K |