4JYQ
DHP-CO crystal structure
Experimental procedure
| Experimental method | SINGLE WAVELENGTH |
| Source type | SYNCHROTRON |
| Source details | APS BEAMLINE 14-ID-B |
| Synchrotron site | APS |
| Beamline | 14-ID-B |
| Temperature [K] | 293 |
| Detector technology | CCD |
| Collection date | 2012-07-18 |
| Detector | MAR CCD 165 mm |
| Spacegroup name | P 21 21 21 |
| Unit cell lengths | 58.900, 68.590, 69.350 |
| Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
| Resolution | 48.770 - 1.800 |
| R-factor | 0.16137 |
| Rwork | 0.159 |
| R-free | 0.21245 |
| Structure solution method | MOLECULAR REPLACEMENT |
| RMSD bond length | 0.022 |
| RMSD bond angle | 1.959 |
| Data reduction software | Precognition |
| Phasing software | PHASES |
| Refinement software | REFMAC (5.5.0109) |
Data quality characteristics
| Overall | Outer shell | |
| Low resolution limit [Å] | 100.000 | 1.880 |
| High resolution limit [Å] | 1.800 | 1.800 |
| Number of reflections | 17491 | |
| Completeness [%] | 67.3 | 25.55 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 | VAPOR DIFFUSION, HANGING DROP | 6 | 277 | details 0.2 M Ammonium Sulfate, 29% w/v PEG 8000 , pH 6, VAPOR DIFFUSION, HANGING DROP, temperature 277K |
