4JUP
Dimeric structure of CARMA1 CARD
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | PAL/PLS BEAMLINE 4A |
Synchrotron site | PAL/PLS |
Beamline | 4A |
Temperature [K] | 110 |
Detector technology | CCD |
Collection date | 2012-08-12 |
Detector | ADSC QUANTUM 4r |
Wavelength(s) | 0.999 |
Spacegroup name | P 21 21 21 |
Unit cell lengths | 45.887, 53.863, 92.802 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 41.130 - 3.200 |
R-factor | 0.2646 |
Rwork | 0.259 |
R-free | 0.38756 |
Structure solution method | MOLECULAR REPLACEMENT |
RMSD bond length | 0.015 |
RMSD bond angle | 1.632 |
Data reduction software | HKL-2000 |
Data scaling software | HKL-2000 |
Phasing software | PHASES |
Refinement software | REFMAC (5.5.0102) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 50.000 | 3.310 |
High resolution limit [Å] | 3.200 | 3.200 |
Number of reflections | 5890 | |
Completeness [%] | 12.0 | 96.6 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 6.5 | 293 | 30% PEG 5000 MME, 0.2M Ammonium sulfate, 0.1M sodium acetate pH 6.5, VAPOR DIFFUSION, HANGING DROP, temperature 293K |