4JTV
Crystal structure of 2009 pandemic influenza virus hemagglutinin complexed with human receptor analogue LSTc
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | SSRF BEAMLINE BL17U |
Synchrotron site | SSRF |
Beamline | BL17U |
Temperature [K] | 100 |
Detector technology | CCD |
Collection date | 2010-03-10 |
Detector | MARMOSAIC 225 mm CCD |
Wavelength(s) | 1.0000 |
Spacegroup name | P 1 |
Unit cell lengths | 66.722, 117.321, 117.393 |
Unit cell angles | 61.78, 81.82, 77.42 |
Refinement procedure
Resolution | 38.391 - 2.997 |
R-factor | 0.2264 |
Rwork | 0.224 |
R-free | 0.27540 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 3al4 |
RMSD bond length | 0.011 |
RMSD bond angle | 1.135 |
Data reduction software | HKL-2000 |
Data scaling software | HKL-2000 |
Phasing software | PHASER |
Refinement software | PHENIX ((phenix.refine: 1.5_2)) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 50.000 | 3.110 |
High resolution limit [Å] | 2.997 | 3.000 |
Number of reflections | 53767 | |
Completeness [%] | 88.8 | 59.9 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 6.5 | 291 | 10% PEG6000, 5% MPD, 0.1M MES, pH 6.5, VAPOR DIFFUSION, HANGING DROP, temperature 291K |