4JRX
Crystal Structure of CA5 TCR-HLA B*3505-LPEP complex
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | AUSTRALIAN SYNCHROTRON BEAMLINE MX2 |
Synchrotron site | Australian Synchrotron |
Beamline | MX2 |
Temperature [K] | 100 |
Detector technology | CCD |
Collection date | 2011-03-29 |
Detector | ADSC QUANTUM 315r |
Wavelength(s) | 0.956 |
Spacegroup name | P 1 21 1 |
Unit cell lengths | 55.100, 78.408, 105.339 |
Unit cell angles | 90.00, 93.06, 90.00 |
Refinement procedure
Data quality characteristics
Overall | Inner shell | Outer shell | |
Low resolution limit [Å] | 19.800 | 2.500 | |
High resolution limit [Å] | 2.300 | 10.000 | 2.300 |
Rmerge | 0.099 | 0.063 | 0.505 |
Rmeas | 0.068 | 0.548 | |
Number of reflections | 39947 | 457 | 8770 |
<I/σ(I)> | 13.2 | 28.4 | 3.98 |
Completeness [%] | 99.8 | 86.7 | 100 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 6.7 | 298 | 16% PEG 3350, 0.2M KI, 0.1M Na-cacodylate pH 6.7, vapor diffusion, hanging drop, temperature 298K |