4JRC
Distal Stem I region from G. kaustophilus glyQS T box RNA
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | CHESS BEAMLINE A1 |
Synchrotron site | CHESS |
Beamline | A1 |
Temperature [K] | 100 |
Detector technology | CCD |
Collection date | 2012-07-01 |
Detector | ADSC QUANTUM 210 |
Wavelength(s) | 0.9767 |
Spacegroup name | C 1 2 1 |
Unit cell lengths | 116.461, 41.511, 90.417 |
Unit cell angles | 90.00, 106.76, 90.00 |
Refinement procedure
Resolution | 20.140 - 2.673 |
R-factor | 0.2051 |
Rwork | 0.201 |
R-free | 0.24270 |
Structure solution method | SAD |
RMSD bond length | 0.001 |
RMSD bond angle | 0.409 |
Data reduction software | DENZO |
Data scaling software | SCALEPACK |
Phasing software | SOLVE |
Refinement software | PHENIX (1.8.1_1168) |
Data quality characteristics
Overall | Inner shell | Outer shell | |
Low resolution limit [Å] | 35.000 | 35.000 | 2.700 |
High resolution limit [Å] | 2.650 | 7.170 | 2.650 |
Rmerge | 0.068 | 0.026 | 0.484 |
Number of reflections | 11578 | ||
<I/σ(I)> | 10.9 | 47.56 | 1.808 |
Completeness [%] | 97.2 | 96.3 | 82.7 |
Redundancy | 3.6 | 3.4 | 3.1 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 6 | 291 | 80mM NaCl, 12mM KCl, 20mM MgCl2, 40mM sodium cacodylate, 12mM spermine, 28% 2-methyl-1,3 propanediol, pH 6.0, VAPOR DIFFUSION, HANGING DROP, temperature 291K |