4JJY
Alix V domain
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | ALS BEAMLINE 4.2.2 |
Synchrotron site | ALS |
Beamline | 4.2.2 |
Temperature [K] | 100 |
Detector technology | CCD |
Collection date | 2011-11-30 |
Detector | NOIR-1 |
Wavelength(s) | 0.976 |
Spacegroup name | I 2 3 |
Unit cell lengths | 223.770, 223.770, 223.770 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 39.557 - 6.503 |
R-factor | 0.2107 |
Rwork | 0.203 |
R-free | 0.28320 |
Structure solution method | SAD |
RMSD bond length | 0.002 |
RMSD bond angle | 0.550 |
Data reduction software | d*TREK |
Data scaling software | d*TREK |
Phasing software | PHENIX |
Refinement software | PHENIX ((phenix.refine: 1.8.1_1168)) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 39.560 | 6.730 |
High resolution limit [Å] | 6.500 | 6.500 |
Rmerge | 0.061 | 0.748 |
Number of reflections | 3774 | |
<I/σ(I)> | 23.3 | 2.1 |
Completeness [%] | 100.0 | 100 |
Redundancy | 21.41 | 22.27 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 5 | 277 | 0.1 M sodium citrate pH 5, 6-8% PEG 8000, 5-10% ethylene glycol, VAPOR DIFFUSION, HANGING DROP, temperature 277K |