4JI2
Crystal Structure of 30S ribosomal subunit from Thermus thermophilus
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | APS BEAMLINE 24-ID-C |
Synchrotron site | APS |
Beamline | 24-ID-C |
Temperature [K] | 100 |
Detector technology | CCD |
Collection date | 2011-08-03 |
Detector | ADSC QUANTUM 315 |
Wavelength(s) | 0.98 |
Spacegroup name | P 41 21 2 |
Unit cell lengths | 402.447, 402.447, 174.411 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 48.335 - 3.640 |
R-factor | 0.1582 |
Rwork | 0.155 |
R-free | 0.21130 |
Structure solution method | FOURIER SYNTHESIS |
RMSD bond length | 0.013 |
RMSD bond angle | 1.915 |
Data scaling software | XSCALE |
Phasing software | PHENIX (dev_1119) |
Refinement software | PHENIX (dev_1119) |
Data quality characteristics
Overall | Inner shell | Outer shell | |
Low resolution limit [Å] | 50.000 | 50.000 | 3.860 |
High resolution limit [Å] | 3.640 | 10.690 | 3.640 |
Rmerge | 0.102 | 0.046 | 0.709 |
Number of reflections | 157605 | 6415 | 24166 |
<I/σ(I)> | 10.15 | 28.68 | 1.84 |
Completeness [%] | 98.9 | 95.1 | 95.2 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 6.5 | 277 | MPD , pH 6.5, VAPOR DIFFUSION, HANGING DROP, temperature 277K |