4JGZ
Crystal structure of human coxsackievirus A16 uncoating intermediate (space group I222)
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | DIAMOND BEAMLINE I03 |
Synchrotron site | Diamond |
Beamline | I03 |
Temperature [K] | 294 |
Detector technology | PIXEL |
Collection date | 2012-04-30 |
Detector | DECTRIS PILATUS 6M |
Wavelength(s) | 0.97620 |
Spacegroup name | I 2 2 2 |
Unit cell lengths | 338.400, 360.200, 366.000 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 49.460 - 3.000 |
R-factor | 0.286 |
Rwork | 0.286 |
R-free | 0.31100 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 3vbr |
RMSD bond length | 0.007 |
RMSD bond angle | 1.400 |
Data reduction software | HKL-2000 |
Data scaling software | SCALEPACK |
Phasing software | CNS |
Refinement software | CNS |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 50.000 | 3.110 |
High resolution limit [Å] | 3.000 | 3.000 |
Rmerge | 0.459 | |
Number of reflections | 110576 | |
<I/σ(I)> | 1.1 | 0.3 |
Completeness [%] | 25.1 | 11.5 |
Redundancy | 1.1 | 1.1 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, SITTING DROP | 7 | 294 | 1.0 M to 0.75 M lithium sulfate monohydrate, 4-6% PEG6000, pH 7.0, VAPOR DIFFUSION, SITTING DROP, temperature 294K |
1 | VAPOR DIFFUSION, SITTING DROP | 7 | 294 | 1.0 M to 0.75 M lithium sulfate monohydrate, 4-6% PEG6000, pH 7.0, VAPOR DIFFUSION, SITTING DROP, temperature 294K |