4JG4

Ligand concentration regulates the pathways of coupled protein folding and binding

Experimental procedure

Experimental method	SINGLE WAVELENGTH
Source type	ROTATING ANODE
Source details	RIGAKU FR-E+ DW
Temperature [K]	100
Detector technology	IMAGE PLATE
Detector	RIGAKU
Spacegroup name	P 64
Unit cell lengths	83.152, 83.152, 32.236
Unit cell angles	90.00, 90.00, 120.00

Refinement procedure

Resolution	24.017 - 2.296
R-factor	0.2161
Rwork	0.213
R-free	0.24920
RMSD bond length	0.010
RMSD bond angle	1.488
Data reduction software	HKL-3000
Data scaling software	HKL-3000
Refinement software	PHENIX ((phenix.refine: dev_1111))

Data quality characteristics

	Overall	Outer shell
Low resolution limit [Å]	24.020	2.340
High resolution limit [Å]	2.300	2.300
Number of reflections	5545
<I/σ(I)>	44.3	11.9
Completeness [%]	94.4	78.6
Redundancy	8.9	7.6

Crystallization Conditions

crystal ID	method	pH	temperature	details
1