4JFB
Crystal structure of OmpF in C2 with tNCS
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | ESRF BEAMLINE ID23-1 |
Synchrotron site | ESRF |
Beamline | ID23-1 |
Detector technology | CCD |
Collection date | 2012-07-15 |
Detector | ADSC QUANTUM 315 |
Wavelength(s) | 0.97 |
Spacegroup name | C 1 2 1 |
Unit cell lengths | 161.910, 110.880, 226.140 |
Unit cell angles | 90.00, 104.46, 90.00 |
Refinement procedure
Resolution | 68.570 - 3.801 |
R-factor | 0.2644 |
Rwork | 0.262 |
R-free | 0.31430 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 2zfg |
RMSD bond length | 0.006 |
RMSD bond angle | 1.097 |
Data reduction software | MOSFLM |
Data scaling software | Aimless |
Phasing software | PHASER |
Refinement software | PHENIX ((phenix.refine: 1.8.1_1168)) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 68.570 | 3.940 |
High resolution limit [Å] | 3.800 | 3.800 |
Number of reflections | 32150 | |
Completeness [%] | 83.6 | 28.55 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 8 | 293 | 18-22% PEG 1500, 5-10% 2-Methyl-2,4-pentanediol, 0.1M Tris-HCl pH 8, VAPOR DIFFUSION, HANGING DROP, temperature 293K |
1 | VAPOR DIFFUSION, HANGING DROP | 8 | 293 | 18-22% PEG 1500, 5-10% 2-Methyl-2,4-pentanediol, 0.1M Tris-HCl pH 8, VAPOR DIFFUSION, HANGING DROP, temperature 293K |