4JB2
Rhodopseudomonas palustris (strain CGA009) Rp1789
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | DIAMOND BEAMLINE I02 |
Synchrotron site | Diamond |
Beamline | I02 |
Temperature [K] | 100 |
Detector technology | CCD |
Collection date | 2012-03-04 |
Detector | ADSC QUANTUM 4 |
Wavelength(s) | 0.91840 |
Spacegroup name | P 21 21 21 |
Unit cell lengths | 42.930, 66.430, 100.520 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 40.080 - 2.100 |
R-factor | 0.17686 |
Rwork | 0.174 |
R-free | 0.22769 |
Structure solution method | MOLECULAR REPLACEMENT |
RMSD bond length | 0.019 |
RMSD bond angle | 1.810 |
Data reduction software | XDS |
Data scaling software | XSCALE |
Phasing software | PHASER |
Refinement software | REFMAC (5.5.0110) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 43.000 | 2.150 |
High resolution limit [Å] | 2.100 | 2.100 |
Completeness [%] | 98.0 | 99.3 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 4.5 | 290 | 0.1M sodium acetate pH 4.5, 25% w/v PEG3350, VAPOR DIFFUSION, HANGING DROP, temperature 290K |