4J9V
Crystal Structure of the TrkA Gating ring bound to ATP-gamma-S
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | ALS BEAMLINE 8.2.2 |
Synchrotron site | ALS |
Beamline | 8.2.2 |
Temperature [K] | 100 |
Detector technology | CCD |
Collection date | 2012-09-23 |
Detector | ADSC QUANTUM 315r |
Wavelength(s) | 0.99997 |
Spacegroup name | P 61 2 2 |
Unit cell lengths | 109.324, 109.324, 337.656 |
Unit cell angles | 90.00, 90.00, 120.00 |
Refinement procedure
Resolution | 49.170 - 3.051 |
R-factor | 0.2144 |
Rwork | 0.211 |
R-free | 0.27200 |
Structure solution method | MOLECULAR REPLACEMENT |
RMSD bond length | 0.006 |
RMSD bond angle | 1.021 |
Data reduction software | DENZO |
Data scaling software | SCALEPACK |
Phasing software | PHASER |
Refinement software | PHENIX (1.8.1_1168) |
Data quality characteristics
Overall | Inner shell | Outer shell | |
Low resolution limit [Å] | 50.000 | 50.000 | 3.100 |
High resolution limit [Å] | 3.050 | 8.270 | 3.050 |
Rmerge | 0.103 | 0.036 | 0.889 |
Number of reflections | 23765 | ||
<I/σ(I)> | 8.6 | ||
Completeness [%] | 100.0 | 100 | 100 |
Redundancy | 11.7 | 10.1 | 12.1 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, SITTING DROP | 9 | 298 | 30% PEG 400, 100 mM Glycine, 200 mM MgSO4, pH 9.0, VAPOR DIFFUSION, SITTING DROP, temperature 298K |