4J8B
Crystal structure of alpha-COP/Emp47p complex
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | APS BEAMLINE 24-ID-E |
Synchrotron site | APS |
Beamline | 24-ID-E |
Detector technology | CCD |
Detector | ADSC QUANTUM 315 |
Spacegroup name | P 21 21 21 |
Unit cell lengths | 49.743, 81.958, 87.227 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 59.729 - 1.878 |
R-factor | 0.1789 |
Rwork | 0.176 |
R-free | 0.21720 |
Structure solution method | MOLECULAR REPLACEMENT |
RMSD bond length | 0.008 |
RMSD bond angle | 1.356 |
Refinement software | PHENIX ((phenix.refine: 1.8_1069)) |
Data quality characteristics
Overall | |
Low resolution limit [Å] | 77.105 |
High resolution limit [Å] | 1.878 |
Number of reflections | 29390 |
Completeness [%] | 98.8 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 |