4J87
Crystal structure of alpha-COP
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | APS BEAMLINE 24-ID-E |
Synchrotron site | APS |
Beamline | 24-ID-E |
Detector technology | CCD |
Detector | ADSC QUANTUM 315 |
Spacegroup name | P 21 21 21 |
Unit cell lengths | 37.432, 53.614, 157.961 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 50.769 - 1.670 |
R-factor | 0.1686 |
Rwork | 0.167 |
R-free | 0.19150 |
Structure solution method | MOLECULAR REPLACEMENT |
RMSD bond length | 0.009 |
RMSD bond angle | 1.257 |
Refinement software | PHENIX ((phenix.refine: 1.8_1069)) |
Data quality characteristics
Overall | |
Low resolution limit [Å] | 50.769 |
High resolution limit [Å] | 1.670 |
Number of reflections | 35377 |
Completeness [%] | 98.2 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 |