4J84
Crystal structure of beta'-COP/Scyl1 complex
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | APS BEAMLINE 24-ID-E |
Synchrotron site | APS |
Beamline | 24-ID-E |
Detector technology | CCD |
Detector | ADSC QUANTUM 315 |
Spacegroup name | P 1 |
Unit cell lengths | 42.554, 46.155, 84.300 |
Unit cell angles | 81.46, 81.96, 69.47 |
Refinement procedure
Resolution | 39.952 - 1.473 |
R-factor | 0.1884 |
Rwork | 0.188 |
R-free | 0.20790 |
Structure solution method | MOLECULAR REPLACEMENT |
RMSD bond length | 0.006 |
RMSD bond angle | 1.171 |
Refinement software | PHENIX ((phenix.refine: 1.7.3_928)) |
Data quality characteristics
Overall | |
Low resolution limit [Å] | 50.000 |
High resolution limit [Å] | 1.470 |
Number of reflections | 93130 |
Completeness [%] | 93.5 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 |