4J82
Crystal structure of beta'-COP/Insig-2 complex
Experimental procedure
| Experimental method | SINGLE WAVELENGTH |
| Source type | SYNCHROTRON |
| Source details | APS BEAMLINE 24-ID-E |
| Synchrotron site | APS |
| Beamline | 24-ID-E |
| Detector technology | CCD |
| Detector | ADSC QUANTUM 315 |
| Spacegroup name | P 1 |
| Unit cell lengths | 49.056, 48.894, 76.027 |
| Unit cell angles | 88.83, 89.15, 62.91 |
Refinement procedure
| Resolution | 43.674 - 1.461 |
| R-factor | 0.1695 |
| Rwork | 0.169 |
| R-free | 0.21220 |
| Structure solution method | MOLECULAR REPLACEMENT |
| RMSD bond length | 0.006 |
| RMSD bond angle | 1.120 |
| Refinement software | PHENIX ((phenix.refine: 1.7.3_928)) |
Data quality characteristics
| Overall | |
| Low resolution limit [Å] | 76.010 |
| High resolution limit [Å] | 1.461 |
| Number of reflections | 102387 |
| Completeness [%] | 95.9 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 |
