4J82
Crystal structure of beta'-COP/Insig-2 complex
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | APS BEAMLINE 24-ID-E |
Synchrotron site | APS |
Beamline | 24-ID-E |
Detector technology | CCD |
Detector | ADSC QUANTUM 315 |
Spacegroup name | P 1 |
Unit cell lengths | 49.056, 48.894, 76.027 |
Unit cell angles | 88.83, 89.15, 62.91 |
Refinement procedure
Resolution | 43.674 - 1.461 |
R-factor | 0.1695 |
Rwork | 0.169 |
R-free | 0.21220 |
Structure solution method | MOLECULAR REPLACEMENT |
RMSD bond length | 0.006 |
RMSD bond angle | 1.120 |
Refinement software | PHENIX ((phenix.refine: 1.7.3_928)) |
Data quality characteristics
Overall | |
Low resolution limit [Å] | 76.010 |
High resolution limit [Å] | 1.461 |
Number of reflections | 102387 |
Completeness [%] | 95.9 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 |