4J78
Crystal structure of beta'-COP/Emp47p complex
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | APS BEAMLINE 24-ID-E |
Synchrotron site | APS |
Beamline | 24-ID-E |
Detector technology | CCD |
Detector | ADSC QUANTUM 315 |
Spacegroup name | C 1 2 1 |
Unit cell lengths | 75.187, 51.220, 85.137 |
Unit cell angles | 90.00, 101.60, 90.00 |
Refinement procedure
Resolution | 36.825 - 1.478 |
R-factor | 0.1426 |
Rwork | 0.142 |
R-free | 0.16280 |
Structure solution method | MOLECULAR REPLACEMENT |
RMSD bond length | 0.006 |
RMSD bond angle | 1.251 |
Refinement software | PHENIX ((phenix.refine: 1.8_1069)) |
Data quality characteristics
Overall | |
Low resolution limit [Å] | 83.397 |
High resolution limit [Å] | 1.478 |
Number of reflections | 51789 |
Completeness [%] | 97.6 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 |